Conventional batch cell and FASTFLOT pilot plant studies of reverse flotation of coarse marcasite and pyrite (100 - 400 m) to reduce the sulphidic sulphur content of a rutile concentrate, were undertaken. The batch cell experiments found no significant improvement in sulphur removal with acid wash and copper activation of marcasite and pyrite. Batch cell trials also identified potential difficulties of conventional mechanical cell plants operated at 40 per cent w/w solids. The FASTFLOT 250 B-2 pilot plant trials indicated that with a 0.6 - 0.7 per cent w/w feed sulphur content, target product grade can be met on a routine basis by a three-stage FASTFLOT plant floating coarse marcasite and pyrite. The trials found that 150 g/t PAX dosage and 15 minutes conditioning time are adequate reagentisation for 40 per cent w/w solids feed to the FASTFLOT plant.