Recovery of metallic values from lean-grade raw materials as well as from secondary/intermediate industrial products is of immense importance to a country like India which is not endowed with extensive sources of copper and nickel. The results of a few studies carried out in this area are described in Part-I and Part-II in this article. A novel anode casting system, specially designed for a small copper refinery which had been set up to produce copper wire bars/rods is described briefly in Part-III.