The presence of cyanide soluble copper in gold ores can give rise to serious operational and economical difficulties in CIP and CIL operations. Cyanide consumption can result in the ore being uneconomic to treat by conventional means. Loading of copper onto carbon can also have deleterious effects on gold recovery and subsequent stripping and bullion recovery. The recovery of gold from high copper ores has been previously reviewed by Muir, LaBrooy and Cao (1989). Work undertaken for Mt Gibson Gold Project by Australian Mining Advisors with the assistance of the Chemistry Centre (WA) resulted in the patenting of a process and subsequent construction of a plant at Mt Gibson to overcome some of the difficulties encountered with copper. This paper discusses some of the work which was undertaken during laboratory investigations prior to commissioning of the plant and some further considerations for the treatment of high copper gold ores.