A key parameter affecting the performance of gravity thickeners in hydrometallurgical processing operations is the aggregation state of the feed after the addition of a flocculant. New procedures which measure the settling ratelsize relationship and the size distribution of aggregates in their process liquors have been used to quantify the aggregation state of the feedwell, overflow and underflow streams in a tailings thickener. The data obtained have been related to the thickener's operation and to a change in the flocculant dosage. A comparison is also made between the settling rate/size relationships determined with these new procedures and the mud-line settling rates from cylinder tests.