The Vanderbijl Park sinter plant in South Africa was investigated to determine the reason for the production of very fine sinter not acceptable as feedstock for the blast furnace. A procedure was designed to generate representative samples and to prepare the samples for chemical and mineralogical analyses._x000D_
Results from a mineral analyser showed that the samples are extremely heterogeneous and therefore the sampling and sample preparation methods had to be tested in order to produce representative samples. The high production capacity at the sinter plant could also give rise to sampling errors. The method designed involved sampling of the conveyor belt at the sinter plant every four hours for the duration of three days. The samples were then milled and split into smaller sections appropriate for analysis. X-Ray diffraction (XRD) and X-Ray fluorescence (XRF) analyses were conducted on the samples. The results showed a standard deviation of less then one per cent, which indicates that the samples were representative and that the method used was therefore adequate._x000D_
Systematic differences in the phase proportions between normal and fine sinter samples were detected, with the fine sinter containing more haematite than the normal sinter. The sampling method employed gives added confidence that the differences are real.