Pilot plant work has played a major role in the process development and design phase of the Iscor Heavy Minerals project. The pilot plant campaigns have been aimed at three process areas, namely primary beneficiation (wet gravity circuits), heavy mineral separation and ilmenite smelting. A process development structure was put in place, and the various pilot plants designed and built. A number of pilot campaigns were conducted during the project phase since 1995, and most of the key objectives were achieved. Various other valuable lessons' were learnt, and were incorporated in the full-scale plant designs, or used to change operating philosophies, equipment choices et cetera. The cost and durations of the pilot runs were significant, and an analysis indicated that the major risk and technology area of smelting has contributed more than 70 per cent of the total cost.