During the development of a mining project, samples are taken for metallurgical tests. The sample can be a composite sample made of material coming from a selection of various drilling products or a sample coming from a mining test. This sample can represent several tonnes of material which are analysed and split to be used in various tests.In the current case, a composite sample is dedicated to semi-autogenous grinding (SAG) pilot plant tests. The property of interest is then the size distribution of the material. The sample is mixed and a subsample is taken to measure the size distribution which is considered as the feed size distribution. Then the remaining material of the sample is divided in several subsamples for batch grinding tests at different operating conditions. The product of each grinding test is then analysed to measure its size distribution.The grinding performances are analysed at the light of the measured size distributions for feed and product. But what is the accuracy of the measurement of these size distributions? What is the variability of the feed knowing each feed is just a subsample of the initial sample?The Pierre Gy theory of sampling answers these questions.The current paper presents, through a real example, the calculation of the measurement error of the size distributions and the variability of the feed between the different tests. The uncertainties of the grinding performances are then calculated and their impact on the results interpretation is then analysed.CITATION:Brochot, S, 2012. Sampling for grinding pilot plant test - the effect of size distribution variability, in Proceedings Sampling 2012 , pp 127-134 (The Australasian Institute of Mining and Metallurgy: Melbourne).